HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 65463282, compound → HCID 71526661, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 65463282 | HCID 65463282 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526661 | HCID 71526661 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 69, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 50 mg, 0.21 mmol) and 2-amino-3-cyclobutyl-propan-1-ol (38.7 mg, 0.3 mmol) as starting materials and isolated (30 mg, 41%) as white solid; LC-MS (UV peak area, ESI) 99.69%, 346.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-4b8a035c0a22412281f527916244460c |
| Source note | uspto-grants-2016_08 |