HuagongsheHuagongshe Chemistry Print Report · For research reference only
173336-86-2 → HCID 71526664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 173336-86-2 | HCID 75421022 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid | HCID 86682331 | — |
| Product | HCID 71526664 | HCID 71526664 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 6, using 5-cyclopropyl-6-cyclopropylmethoxy-pyrazine-2-carboxylic acid (Example 10 g, 50 mg, 0.21 mmol) and 3-amino-3-methyl-butanamide hydrochloride (1:1) (CAN 173336-86-2, 35.8 mg, 0.235 mmol) as starting materials and isolated (56 mg, 79%) as light yellow solid; LC-MS (UV peak area, ESI) 100%, 333.1926 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403808B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-f0a14746e0704c239097f908a8d9136e |
| Source note | uspto-grants-2016_08 |