HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57523965, compound → HCID 57524056, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57523965 | HCID 57523965 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57524056 | HCID 57524056 | — |
Reaction Steps
A mixture of (E)-N-(1-(3-(4-chlorophenyl)-1-cyanopent-1-en-3-yl)-1H-indazol-4-yl)methanesulfonamide (60 mg) and 10% Pd/C in EA (4 mL) was stirred at room temperature under H2 atmosphere for 16 h. The mixture was filtered and evaporated to give the title compound as a pale yellow solid. LC/MS m/z=417.2[M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403807B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-decdd1a6be33446b8e2d167e9bea02c0 |
| Source note | uspto-grants-2016_08 |