HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 118364825, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 131736510 | HCID 131736510 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 118364825 | HCID 118364825 | — |
Reaction Steps
3-((6-(1-methyl-1H-pyrazol-4-yl)-1H-[1,2,3]triazolo[4,5-b]pyrazin-1-yl)methyl)piperidine-1-carboxylate (0.45 g, 0.89 mmol) was dissolved in CH2Cl2 (5 ml), and then TFA (5 ml) was added, followed by stirring at room temperature overnight. After the completion of the reaction, the reaction mixture was concentrated under reduced pressure, and the next reaction was advanced without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09403831B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-9bea9762d6394bed83c03d1ee84365ef |
| Source note | uspto-grants-2016_08 |