HCID 102287610, compound → HCID 118513297, compound

Participants

Reaction Steps

To a solution of N-(2-allyl-4-(trifluoromethoxy)phenyl)acrylamide (15 g, 55.3 mmol) in DCM (800 ml) was added Zhan catalyst I (2.0 g, 2.77 mmol) and the mixture was stirred at room temperature for 3 hrs. The resulting mixture was concentrated under reduced pressure to give a crude solid that was recrystallized from ethyl acetate to give the title compound.

Provenance & Evidence