Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Hexafluoropropylene | HCID 8302 | — |
| Reactant | Trimethylene carbonate | HCID 123834 | — |
| Product | HCID 86641050 | HCID 86641050 | — |
Reaction Steps
Example 6 was prepared by combining 1,3-dioxan-2-one (240 g, 2.35 moles) (Richman Chemical Inc., Lower Gwynedd, Pa.) with benzoyl peroxide (5 g, 0.02 moles) in a 600 mL Parr reactor. The reactor was heated to 73° C. and hexafluoropropene (16 g, 0.1066 moles) was fed into the reactor over a 24 h period. The reactor was maintained at the set temperature for an additional 24 h. The reactor contents were collected and analyzed by GC/MS.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09406977B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-db4e03d31f65447b9e6f67f57d32898d |
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| Source note | uspto-grants-2016_08 |
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