Benzoyl Peroxide → HCID 86641050, compound
Reaction equation
[O:1]1[CH2:6][CH2:5][CH2:4][O:3][C:2]1=[O:7].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1.[F:26][C:27]([F:34])([F:33])[C:28]([F:32])=[C:29]([F:31])[F:30]>>[F:30][C:29]([CH:6]1[CH2:5][CH2:4][O:3][C:2](=[O:7])[O:1]1)([F:31])[CH:28]([F:32])[C:27]([F:34])([F:33])[F:26]Participants
4
Conditions
- Temperature
- 73 °C
Procedure
Example 6 was prepared by combining 1,3-dioxan-2-one (240 g, 2.35 moles) (Richman Chemical Inc., Lower Gwynedd, Pa.) with benzoyl peroxide (5 g, 0.02 moles) in a 600 mL Parr reactor. The reactor was heated to 73° C. and hexafluoropropene (16 g, 0.1066 moles) was fed into the reactor over a 24 h period. The reactor was maintained at the set temperature for an additional 24 h. The reactor contents were collected and analyzed by GC/MS.
Workup
- customExample 6 was prepared
- temperatureThe reactor was maintained at the set temperature for an additional 24 h
- customThe reactor contents were collected
Sources & evidence
- ORD record
- ord-db4e03d31f65447b9e6f67f57d32898d
- Source dataset
- uspto-grants-2016_08
- Patent number
- US09406977B2
Reaction notes
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