HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86652358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 58213539 | HCID 58213539 | — |
| Product | HCID 86652358 | HCID 86652358 | — |
Reaction Steps
A solution of 4-(2-(5-amino-8-methylbenzo[f][1,7]naphthyridin-2-yl)ethyl)-3-methylbenzoic acid (from the previous step) in thionyl chloride was stirred at 60° C. for 3 hour. After cooling to ambient temperature, the reaction mixture was concentrated en vaccuo. The crude material was used for next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09408907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-030bb7bfadef40d197d26726f45b6cfc |
| Source note | uspto-grants-2016_08 |