HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 5324398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Daidzein | HCID 5281708 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 5324398 | HCID 5324398 | — |
Reaction Steps
20 ml of a mixture of concentrated sulfuric acid and nitric acid (3:1) are added dropwise to a solution of 1 g of daidzein in 200 ml of dry ethanol at room temperature while stirring vigorously. The mixture is stirred for another 2 hours, and 400 ml of water are then added. The compound precipitates, is filtered off with suction and washed with water until neutral. The yellow product is recrystallized from alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409859B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-0d98c916f9634535a4978387a63ea6e0 |
| Source note | uspto-grants-2016_08 |