HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68372404, compound → HCID 70810769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68372404 | HCID 68372404 | — |
| Solvent | Dichloromethane cyclohexane | HCID 21916607 | — |
| Product | HCID 70810769 | HCID 70810769 | — |
Reaction Steps
(1,4-dimethoxy-3-methylnaphthalen-2-yl)(2-fluoro-4-(trifluoromethyl) phenyl)methanone LJ123 (23 mg, 0.060 mmol) was used as a starting material and treated according to general procedure 12.1. The resulting yellow oil was purified through flash chromatography (DCM:Cyclohexane 1:1). The product was obtained as a yellow solid. Rf(DCM:Cyclohexane 1:1)=0.55. Yield=15 mg (68%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409879B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-d5fda68addbe43998c85ac57c0ad05c3 |
| Source note | uspto-grants-2016_08 |