HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136471032, compound → HCID 122443720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136471032 | HCID 136471032 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 122443720 | HCID 122443720 | — |
Reaction Steps
5,5′-[2-(4,6-Diphenyl-1,3,5-triazinyl)anthracene-9,10-diyl)bisquinolin-8-ol (6.95 g, 10 mmol) is dissolved in acetonitrile (300 ml), and 2.5 M n-butyl-lithium (9.9 ml, 25 mmol) is added. The solution is stirred at room temperature for 1 h. The yellow precipitate is filtered off, washed with acetonitrile and dried in vacuo (5.8 g, 80%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409883B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-5410277e3e924d40a8055da244913982 |
| Source note | uspto-grants-2016_08 |