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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1479934Generated: October 28, 2026

HCID 136471032, compound → HCID 122443720, compound

https://huagongshe.com/reaction/1479934

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 136471032HCID 136471032—
ReactantButyllithiumHCID 178418339—
SolventAcetonitrileHCID 6342—
ProductHCID 122443720HCID 122443720—

Reaction Steps

5,5′-[2-(4,6-Diphenyl-1,3,5-triazinyl)anthracene-9,10-diyl)bisquinolin-8-ol (6.95 g, 10 mmol) is dissolved in acetonitrile (300 ml), and 2.5 M n-butyl-lithium (9.9 ml, 25 mmol) is added. The solution is stirred at room temperature for 1 h. The yellow precipitate is filtered off, washed with acetonitrile and dried in vacuo (5.8 g, 80%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09409883B2
Source datasetuspto-grants-2016_08
ORD IDord-5410277e3e924d40a8055da244913982
Source noteuspto-grants-2016_08