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HRID148

反应详情

EQUATION

反应方程式

HRID 148 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(N)=O
HCID77922

tert-Butyl carbamate

C5H11NO2

结构：O=C(O)c1cc(Cl)nc(Cl)c1
HCID94830

2,6-Dichloroisonicotinic acid

C6H3Cl2NO2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)Nc1cc(C(=O)O)cc(Cl)n1
HCID72212052

未命名化合物

收率 0%

AUXILIARIES

试剂、催化剂与溶剂

4
结构：O=P([O-])([O-])[O-].[K+].[K+].[K+]
试剂HCID62657

Tripotassium phosphate

K3O4P

结构：CC1(C)c2cccc(P(c3ccccc3)c3ccccc3)c2Oc2c(P(c3ccccc3)c3ccccc3)cccc21
催化剂HCID636044

1,1'-(9,9-Dimethyl-9H-xanthene-4,5-diyl)bis(1,1-diphenylphosphine)

C39H32OP2

结构：O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.O=C(/C=C/c1ccccc1)/C=C/c1ccccc1.[Pd].[Pd]
催化剂HCID9811564

Bis(dibenzylideneacetone)palladium

C51H42O3Pd2

结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

CONDITIONS

反应条件

温度
100 °C

PROCEDURE

实验过程

Reagents were mixed in a 25 mL round bottom flask and flushed well with nitrogen - heated at 100 °C for 16 h. The mixture looked dark black. Could not detect any starting material or product! It was discarded.