Hydrochloric Acid → 2-Amino-2-ethyl-N-methyl-butyramide hydrochloride

Participants

Reaction Steps

A mixture of tert-butyl 3-(methylcarbamoyl)pentan-3-ylcarbamate (0.18 g, 0.74 mmol) in 10 ml saturated hydrochloride in ethyl acetate was stirred for 60 min at room temperature. Then the solution was evaporated to dryness to obtain the product (80 mg, 75%) as a light yellow solid. MS (ESI, m/z): 145.2 (M+H+)

Provenance & Evidence