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HRID1480101

反应详情

EQUATION

反应方程式

HRID 1480101 的结构方程式

REACTANTS

反应物

2
结构：CNC(=O)[C@@H](N)C(C)(C)C
HCID445856

(S)-2-Amino-N-methyl-3,3-dimethylbutanamide

C7H16N2O

结构：O=C(O)c1cc(OCC(F)(F)F)c(C2CC2)cn1
HCID90203674

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)[C@@H](NC(=O)c1cc(OCC(F)(F)F)c(C2CC2)cn1)C(C)(C)C
HCID76282720

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 24d, using 5-Cyclopropyl-4-(2,2,2-trifluoro-ethoxy)-pyridine-2-carboxylic acid (Example 48c) and (S)-2-amino-N,3,3-trimethylbutanamide (CAN 89226-12-0) as starting materials and isolated (115 mg, 52%) as a white solid; MS (ESI, m/z): 388.5 (M+H+).

WORKUP

后处理

  1. customisolated (115 mg, 52%) as a white solid