HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-4-chloropyridine → HCID 90204500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-4-chloropyridine | HCID 817696 | — |
| Reactant | (2S)-1,1,1-Trifluoropropan-2-ol | HCID 6999971 | — |
| Product | HCID 90204500 | HCID 90204500 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 78a, using 3-bromo-4-chloropyridine (CAN 36953-42-1) and (S)-1,1,1-trifluoropropan-2-ol (CAN 3539-97-7) as starting materials and isolated (28 g, 82%) as a yellow oil; MS (ESI, m/z): 270.4 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409866B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-b9d6ecc61f1040df815d211b8d316c85 |
| Source note | uspto-grants-2016_08 |