HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoroethanol → HCID 90203478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoroethanol | HCID 9737 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 90203632 | HCID 90203632 | — |
| Product | HCID 90203478 | HCID 90203478 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 123c, using 4-chloro-5-cyclopropyl-pyridine-2-carbonitrile (example 145b), 2-Fluoro-ethanol (CAN 371-62-0) as starting materials and sodium hydride as reagent. The title compound was isolated (267 mg, 68%) as a yellow solid; MS (ESI, m/z): 207.1 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409866B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-f1bcb73b4f7348a9b432e5e17e494b3d |
| Source note | uspto-grants-2016_08 |