HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 90214971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 2-[[5-cyclopropyl-4-[(1S)-2,2,2-trifluoro-1-methyl-ethoxy]pyridine-2-carbonyl]amino]-3,3-dimethyl-butanoic acid | HCID 90203539 | — |
| Product | HCID 90214971 | HCID 90214971 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 112e, using 2-[[5-cyclopropyl-4-[(1S)-2,2,2-trifluoro-1-methyl-ethoxy]pyridine-2-carbonyl]amino]-3,3-dimethyl-butanoic acid (Example 199b) and ammonium chloride as starting materials and isolated (105 mg, 88%); MS (ESI, m/z): 388.6 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409866B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-7eec2bc203494b92ab8d09d17c6b0129 |
| Source note | uspto-grants-2016_08 |