HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178520554, compound → HCID 178520555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178520554 | HCID 178520554 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178520555 | HCID 178520555 | — |
Reaction Steps
A solution of (E)-N-(1-(3-(3,5-dichlorophenyl)acryloyl)piperidin-4-yl)-4-(1H-1,2,3-triazol-4-yl)butanamide (Example 38) (70 mg, 0.160 mmol) in EtOH (6 ml) was allowed to pass through the H cube fitted with a 10% Pt/C catalytic cartridge for 3 hours. The reaction mixture was concentrated under reduced pressure to afford the title product;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409895B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-712cebe819944f94ad98268d73b1784e |
| Source note | uspto-grants-2016_08 |