Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1480464Generated: October 30, 2026

Hydrochloric Acid → HCID 90218956, compound

https://huagongshe.com/reaction/1480464

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86722689HCID 86722689—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 90218956HCID 90218956—

Reaction Steps

A reaction mixture comprising tert-butyl 4-((((3,5-dichlorobenzyl)oxy)carbonyl)amino)piperidine-1-carboxylate (2.01 g, 4.98 mmol) and 4M HCl in dioxane (1.246 ml, 4.98 mmol) in dioxane (16.61 ml) was stirred at room temperature for 1 hour. The resulting mixture was concentrated under reduced pressure. No further purification under taken and the material was dried and taken on to the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09409895B2
Source datasetuspto-grants-2016_08
ORD IDord-3e7c472a67d447c1a38f162c6b5b31a9
Source noteuspto-grants-2016_08