HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89996054, compound → HCID 89996101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89996054 | HCID 89996054 | — |
| Reactant | HCID 90000823 | HCID 90000823 | — |
| Product | HCID 89996101 | HCID 89996101 | 25% |
Reaction Steps
The title compound was prepared according to Example 40 using N-(4-(1-(2-(dimethylamino)ethyl)-1H-pyrazol-4-yl)-2-methoxyphenyl)formamide (Preparation 64) and N-cyclohexyl-2-(methylsulfonyl)pyrido[3,4-d]pyrimidin-8-amine (Preparation 44). The residue was purified by silica gel column chromatography eluting with 0 to 10% MeOH in DCM to give the title compound (26 mg, 25%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-313a608a1da44c31a65d6aac6cc3a151 |
| Source note | uspto-grants-2016_08 |