HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89996011, compound → HCID 73386780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89996011 | HCID 89996011 | — |
| Reactant | HCID 89996126 | HCID 89996126 | — |
| Product | HCID 73386780 | HCID 73386780 | 38% |
Reaction Steps
The title compound was prepared according to Example 40 using N-(2-methoxy-4-(1-methyl-1H-imidazol-5-yl)phenyl)formamide (Preparation 74) and 2-(methylsulfonyl)-N-neopentylpyrido[3,4-d]pyrimidin-8-amine (Preparation 47). The residue was purified by silica gel column chromatography eluting with 0-20% MeOH in EtOAc followed by a second chromatography eluting with 0-10% MeOH in EtOAc to give the title compound (7.5 mg, 38%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-8eb478537b7c4bb389e3c3ba69d2fcf7 |
| Source note | uspto-grants-2016_08 |