HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89996185, compound → HCID 73386776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89996185 | HCID 89996185 | — |
| Reactant | HCID 89996294 | HCID 89996294 | — |
| Product | HCID 73386776 | HCID 73386776 | 52% |
Reaction Steps
The title compound was prepared according to Example 40 using N-(2-methoxy-4-(1-methyl-1H-pyrazol-4-yl)phenyl)formamide (Preparation 56) and 8-(cyclopropylmethoxy)-2-(methylsulfonyl)pyrido[3,4-d]pyrimidine (Preparation 69). The residue was purified by silica gel column chromatography eluting with 0 to 75% EtOAc in cyclohexane to give the title compound (27 mg, 52%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-02649d0911fd4f66ba86d34c5a69f311 |
| Source note | uspto-grants-2016_08 |