Formic Acid → HCID 89996299, compound

Participants

Reaction Steps

A solution of 2-methyl-4-(1-methyl-1H-pyrazol-4-yl)aniline (Preparation 98, 100 mg, 0.534 mmol) in formic acid (3 mL) was heated to reflux for 3 hours. The reaction mixture was concentrated in vacuo. The residue was partitioned between aqueous saturated NaHCO3 solution (30 mL) and EtOAc (30 mL). The aqueous layer was re-extracted with EtOAc (30 mL).

Provenance & Evidence