HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromo-2-methoxypyridin-3-amine → HCID 89996203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromo-2-methoxypyridin-3-amine | HCID 10536137 | — |
| Reactant | 1,5-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole | HCID 42647313 | — |
| Product | HCID 89996203 | HCID 89996203 | — |
Reaction Steps
The title compound was prepared according to the method described for Preparation 158 using 6-bromo-2-methoxypyridin-3-amine and 1,5-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrazole. The crude residue was purified using silica gel column chromatography eluting with 1-10% MeOH/aqueous ammonia (10/1) in DCM.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409907B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-53a46d813acf45dc88af6d24e47f34e3 |
| Source note | uspto-grants-2016_08 |