Potassium Carbonate → HCID 89996215, compound

Participants

Reaction Steps

Potassium carbonate (0.020 g, 0.148 mmol) was added to a solution of 2-methoxy-3-nitro-6-((trimethylsilyl)ethynyl)pyridine (Preparation 201, 0.37 g, 1.478 mmol) in MeOH (3 mL). The reaction mixture was stirred at room temperature for 1 hour. The reaction was concentrated in vacuo and diluted with EtOAc. The solution was washed with water and the organic layer was dried (Na2SO4) and concentrated in vacuo to afford the title compound as a brown solid (248 mg, 94%).

Provenance & Evidence