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HRID1480879

反应详情

EQUATION

反应方程式

HRID 1480879 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)N1CCNCC1
HCID709161

未命名化合物

结构：COc1cc(F)ccc1[N+](=O)[O-]
HCID2779250

5-Fluoro-2-nitroanisole

C7H6FNO3

PRODUCTS

生成物

1
结构：COc1cc(N2CCN(S(C)(=O)=O)CC2)ccc1[N+](=O)[O-]
HCID59860255

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the method described for Preparation 78 using 4-fluoro-2-methoxy-1-nitrobenzene and 1-(methylsulfonyl)piperazine for 96 hours. The residue was purified by silica gel column chromatography eluting with 50-100% DCM in cyclohexanes.

WORKUP

后处理

  1. customThe residue was purified by silica gel column chromatography
  2. washeluting with 50-100% DCM in cyclohexanes