HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2,6-difluorobenzaldehyde → 1-(3-Chloro-2-fluoro-6-methoxyphenyl)prop-2-en-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2,6-difluorobenzaldehyde | HCID 736338 | — |
| Reactant | 3-Chloro-2-fluoro-6-methoxybenzaldehyde | HCID 22139707 | — |
| Product | 1-(3-Chloro-2-fluoro-6-methoxyphenyl)prop-2-en-1-one | HCID 90034457 | — |
Reaction Steps
1-(3-Chloro-2-fluoro-6-methoxyphenyl)prop-2-en-1-one was prepared using a procedure analogous to intermediate 1 except that 3-chloro-2,6-difluorobenzaldehyde was replaced with 3-chloro-2-fluoro-6-methoxybenzaldehyde. 1H NMR (400 MHz, CHLOROFORM-d) δ 7.43-7.36 (m, 1H), 6.75-6.56 (m, 2H), 6.13-6.03 (m, 2H), 3.80 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409908B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-b526583e79d246a9bb36b07b5b8b77a3 |
| Source note | uspto-grants-2016_08 |