HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90011425, compound → HCID 90011543, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90011425 | HCID 90011425 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 90011543 | HCID 90011543 | — |
Reaction Steps
Step-6: 3-Methyl-5-(1-(6-nitropyridin-3-yl)-5-(trifluoromethyl)-1H-pyrazol-3-yl)-1,3,4-oxadiazol-2(3H)-one: The title compound was prepared from step-5 intermediate by following the similar procedure sequentially as described in Step-5 and Step-6 of Intermediate-1. 1HNMR (400 MHz, CDCl3) δ 8.91(d, J=2.5 Hz, 1H), 8.48 (d, J=8.5 Hz, 1H), 8.31(dd, J=2.5 & 8.5 Hz, 1H), 7.37 (s, 1H), 3.53 (s, 3H); ESI-MS (m/z) 398 (M+acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409898B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-d7da622130b34a62bd3af45c6e8f87b7 |
| Source note | uspto-grants-2016_08 |