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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1481494Generated: November 1, 2026

HCID 90011425, compound → HCID 90011543, compound

https://huagongshe.com/reaction/1481494

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 90011425HCID 90011425—
SolventAcetonitrileHCID 6342—
ProductHCID 90011543HCID 90011543—

Reaction Steps

Step-6: 3-Methyl-5-(1-(6-nitropyridin-3-yl)-5-(trifluoromethyl)-1H-pyrazol-3-yl)-1,3,4-oxadiazol-2(3H)-one: The title compound was prepared from step-5 intermediate by following the similar procedure sequentially as described in Step-5 and Step-6 of Intermediate-1. 1HNMR (400 MHz, CDCl3) δ 8.91(d, J=2.5 Hz, 1H), 8.48 (d, J=8.5 Hz, 1H), 8.31(dd, J=2.5 & 8.5 Hz, 1H), 7.37 (s, 1H), 3.53 (s, 3H); ESI-MS (m/z) 398 (M+acetonitrile).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09409898B2
Source datasetuspto-grants-2016_08
ORD IDord-d7da622130b34a62bd3af45c6e8f87b7
Source noteuspto-grants-2016_08