Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1481672Generated: October 30, 2026

HCID 59174704, compound → 3-Methoxyaniline

https://huagongshe.com/reaction/1481672

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59174704HCID 59174704—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
Product3-MethoxyanilineHCID 10824295.3%

Reaction Steps

To a solution of 7 (0.13 g, 0.275 mmol) in methanol (3 mL) was added Pd/C (26 mg, 20% w/w) under N2 atmosphere. Then the reaction mixture was stirred at room temperature under H2 pressure (bladder) for 16 h. It was filtered through celite bed and the filtrate was concentrated to give 8 (0.10 g, 82%) as green solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09409921B2
Source datasetuspto-grants-2016_08
ORD IDord-6570503d385e492783c6254cb1381a40
Source noteuspto-grants-2016_08