HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59174704, compound → 3-Methoxyaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59174704 | HCID 59174704 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Methoxyaniline | HCID 10824 | 295.3% |
Reaction Steps
To a solution of 7 (0.13 g, 0.275 mmol) in methanol (3 mL) was added Pd/C (26 mg, 20% w/w) under N2 atmosphere. Then the reaction mixture was stirred at room temperature under H2 pressure (bladder) for 16 h. It was filtered through celite bed and the filtrate was concentrated to give 8 (0.10 g, 82%) as green solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409921B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-6570503d385e492783c6254cb1381a40 |
| Source note | uspto-grants-2016_08 |