HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4,5-dimethylphenol → 2-Bromo-4-fluoro-5-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4,5-dimethylphenol | HCID 140961 | — |
| Reactant | 4-Fluoro-3-methylphenol | HCID 2737394 | — |
| Product | 2-Bromo-4-fluoro-5-methylphenol | HCID 84672831 | 94% |
Reaction Steps
Prepared in 94% yield from 4-fluoro-3-methylphenol following the procedure for 2-bromo-4,5-dimethylphenol. 1H NMR (400 MHz, CDCl3) δ 7.14 (d, J=8.5 Hz, 3H), 6.86 (d, J=7.0 Hz, 3H), 5.23 (s, 3H), 2.22 (d, J=1.8 Hz, 9H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09409922B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-c45d8c6d6cc146188032c7495ee9f2da |
| Source note | uspto-grants-2016_08 |