HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylcarbodiimide → Thymidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylcarbodiimide | HCID 12734 | — |
| Reactant | 5'-O-(4,4'-Dimethoxytrityl)thymidine | HCID 162419 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Thymidine | HCID 5789 | — |
Reaction Steps
In a nitrogen-replaced glove box, 5′-O-(4,4′-dimethoxytrityl)thymidine and N,N′-diisoproyl carbodiimide were dissolved in dehydrated pyridine with a concentration of 0.1 mol/L and 0.2 mol/L, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09410951B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-fb0d3f7858b44c3f81400cbd6481c089 |
| Source note | uspto-grants-2016_08 |