HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 89691297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | 7-Methoxy-1H-indole | HCID 76660 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 89691297 | HCID 89691297 | 74% |
Reaction Steps
Compound 2 was synthesized from commercially available 7-Methoxyindole using the general procedure and 1-bromobutane to afford 0.51 g (74% yield) as a clear oil. TLC system: 10% EtOAc/90% n-hexanes. Spectral data matched previously reported data.35
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09416103B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-df5c7ca351964cb79d041f61a42fa030 |
| Source note | uspto-grants-2016_08 |