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HRID1482808

反应详情

EQUATION

反应方程式

HRID 1482808 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1ccc(S(=O)(=O)Cl)cc1
HCID82385

Benzoic acid, 4-(chlorosulfonyl)-

C7H5ClO4S

结构：CNc1ccc(C(F)(F)F)cc1
HCID15099755

N-Methyl-4-(trifluoromethyl)aniline

C8H8F3N

PRODUCTS

生成物

1
结构：CN(c1ccc(C(F)(F)F)cc1)S(=O)(=O)c1ccc(C(=O)O)cc1
HCID66762384

未命名化合物

PROCEDURE

实验过程

4-(chlorosulfonyl)benzoic acid (0.5 g, 2.27 mmol) was treated with N-methyl-4-(trifluoromethyl)aniline (1191 mg, 6.80 mmol) using method A to give 4-(N-methyl-N-(4-(trifluoromethyl)phenyl)sulfamoyl)benzoic acid as a white solid. Yield: 385 mg (47%). 1H-NMR: 8.11 (d, J=8.5 Hz, 2H), 7.74 (d, J=8.5 Hz, 2H), 7.66 (d, J=8.5 Hz, 2H), 7.39 (d, J=8.5 Hz, 2H), 3.21 (s, 3H).