HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90134933, compound → HCID 69288665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90134933 | HCID 90134933 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69288665 | HCID 69288665 | — |
Reaction Steps
Dissolve 3-(azidomethyl)-3,4-dihydro-2H-isoquinolin-1-one (1.8 g, 8.9 mmol) in EtOAc (15 mL). Under a nitrogen atmosphere add 10% Pd/C (0.2 g) then stir overnight under a hydrogen atmosphere. Filter reaction mixture through Celite® and wash the Celite® with EtOAc. MS (m/z): 177 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09416138B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-993a92fe52f4474ab7dbf242ac845114 |
| Source note | uspto-grants-2016_08 |