HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropane → HCID 90266390, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 78128152 | HCID 78128152 | — |
| Reactant | HCID 78128153 | HCID 78128153 | — |
| Product | HCID 90266390 | HCID 90266390 | 46.1% |
Reaction Steps
Compound 14b (125 mg, 0.51 mmol), NaH (51 mg, 1.28 mmol) and isopropyl bromide (125 mg, 1.02 mmol) reacted following the synthetic method of compound 14c to afford 67 mg colorless liquid, yield 46%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09416144B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-a88fc92c8d5341aeaa724b0e8bf020c1 |
| Source note | uspto-grants-2016_08 |