Chlorodiisopropylphosphine → HCID 118467176, compound

Participants

Reaction Steps

Title compound (1-2) (5.0 g) was obtained as a colorless powder by the same procedure as in the second step of Example 1, except that the reaction was conducted by use of the toluene solution of the crude product of N-(3-methoxyphenyl) carbazole (4-1) in an amount equivalent to 18.3 mmol, that chlorodiisopropylphosphine was used instead of Cy2PCl, and further that the product was isolated and purified by crystallization from toluene/methanol. Two Steps Overall Isolated Yield: 70.2%.

Provenance & Evidence