HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzyl-4-piperidone → HCID 12718203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzyl-4-piperidone | HCID 19220 | — |
| Reactant | Benzene, 1-iodo-3-(trifluoromethyl)- | HCID 67868 | — |
| Product | HCID 12718203 | HCID 12718203 | 47.3% |
Reaction Steps
Beginning with 3-trifluoromethyl-iodobenzene (3 g) and 1-benzyl-4-piperidone (2.1 g), 1.75 g of the title compound was recovered by the procedure described in preparation 1. MS m/z (rel. intensity, 70 eV) 335 (M+, 29), 244 (22), 146 (19), 91 (bp), 56 (19).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE046117E1 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-6861d7fd0eb841c0af4e0bf97ee4bb1e |
| Source note | uspto-grants-2016_08 |