HCID 89588561, compound → HCID 89588814, compound

Participants

Reaction Conditions

Reaction Steps

5-Benzyloxy-3-(4-bromo-phenyl)-7-fluoro-benzo[f][1,4]oxazepine (830 mg, 1.96 mmol) was dissolved in isopropanol, degassed under reduced pressure and purged with argon. The reaction mixture was heated at 140° C. under microwave irradiation for 1 h. The solvent was then evaporated to dryness to afford the title compound as a solid, which was used without any further purification (750 mg, 90% yield).

Provenance & Evidence