HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methanesulfonate → 3-Amino-2-methyl-5,6-bis(4-methylphenyl)-1,2,4-triazine mesylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methanesulfonate | HCID 4156 | — |
| Reactant | 3-Amino-5,6-bis(4-methylphenyl)-1,2,4-triazine | HCID 58103102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-2-methyl-5,6-bis(4-methylphenyl)-1,2,4-triazine mesylate | HCID 86649732 | — |
Reaction Steps
A mixture of 3-amino-5,6-bis(4-methylphenyl)-1,2,4-triazine (500 mg), methyl methanesulphonate (0.5 cm3) and methanol (10 cm3) was stirred at 40° for 24 hours and then evaporated to dryness. The resulting yellow solid was recrystallised from acetone giving the title compound as pale yellow needles,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422253B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-65ca957cfe3b4b7da334d7247665ae82 |
| Source note | uspto-grants-2016_08 |