Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 75201755 | HCID 75201755 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 75201754 | HCID 75201754 | — |
Reaction Steps
3-benzyl-1-methyl-4-[3-methyl-8-(methylsulfanyl)-[1,2,4]triazolo[4,3-b]pyridazin-6-yl]-1H-pyrazole (32 mg; 0.09 mmol) was dissolved in 1 ml chloroform and was treated with sulfurylchlorid (44 μl; 0.54 mmol). The reaction mixture is stirred for 18 h at 25° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09422290B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-7882f9145087457d8cfea0f37687255a |
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| Source note | uspto-grants-2016_08 |
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