HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1485043Generated: October 31, 2026
(3R)-3-Amino-4-hydroxybutanoic acid → HCID 131736733, compound
https://huagongshe.com/reaction/1485043
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | (3R)-3-Amino-4-hydroxybutanoic acid | HCID 1502076 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131736733 | HCID 131736733 | — |
Reaction Steps
To a solution of L-β-homoserine (1.00 g) in methanol (8.4 mL), a 4 mol/L hydrogen chloride-1,4-dioxane solution (8.4 mL) was added and thereafter the mixture was stirred at 60° C. for 3 hours. The reaction mixture was concentrated under reduced pressure to give the titled compound as a pale yellow oil (1.42 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09422240B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-f5fb4ea35bae423f8338fe1aadb4b25c |
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| Source note | uspto-grants-2016_08 |
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