HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 178502732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | 2-Cyclopropylethan-1-ol | HCID 137642 | — |
| Reactant | HCID 178502733 | HCID 178502733 | — |
| Product | HCID 178502732 | HCID 178502732 | 33.9% |
Reaction Steps
Instead of 2-cyclopropylethanol and 4-hydroxybenzaldehyde, the compound (850 mg) obtained in step (1) above and p-chlorophenol (700 mg) were respectively used and treated by the same technique as in Reference Example 11-1 to give trans-4-(4-chlorophenoxy)-N-methoxy-N-methylcyclohexanecarboxamide as a colorless solid (458 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422240B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-5f8512c94ce1462984e7d6e8349f2b9d |
| Source note | uspto-grants-2016_08 |