HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)benzonitrile → HCID 118113395, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Reactant | p-Cyanobenzyl alcohol | HCID 160549 | — |
| Reactant | 5-Hydroxy-2-(trifluoromethyl)pyridine | HCID 2783388 | — |
| Reactant | 2-Fluoro-5-(trifluoromethyl)pyridine | HCID 5463754 | — |
| Product | HCID 118113395 | HCID 118113395 | — |
Reaction Steps
Instead of 6-(trifluoromethyl)pyridin-3-ol and 4-cyanobenzylbromide, 4-(hydroxymethyl)benzonitrile (1.87 g) and 2-fluoro-5-(trifluoromethyl)pyridine (1.55 g) were respectively used and treated by the same technique as in Reference Example 38-1 to give the titled compound as a pale yellow solid (1.49 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422240B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-384ba5c0d3c44f748ffb32bc3f8d1a6d |
| Source note | uspto-grants-2016_08 |