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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1485122Generated: October 31, 2026

HCID 85923149, compound → HCID 11298265, compound

https://huagongshe.com/reaction/1485122

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 85923149HCID 85923149—
ReactantHCID 178418361HCID 178418361—
CatalystPalladium hydroxideHCID 9942167—
SolventEthyl AcetateHCID 8857—
ProductHCID 11298265HCID 1129826589.1%

Reaction Steps

To a solution in ethyl acetate (20.0 mL) of the compound (634 mg) obtained in step (1) above, 20% palladium hydroxide/carbon (63.0 mg) was added. The mixture was stirred at room temperature for an hour in a hydrogen atmosphere. After passing the reaction mixture through Celite (registered trademark), the filtrate was concentrated under reduced pressure to give the titled compound as a pale yellow oil (320 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09422240B2
Source datasetuspto-grants-2016_08
ORD IDord-4de129214d8849029ad4025fd67ef0c4
Source noteuspto-grants-2016_08