HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 85923149, compound → HCID 11298265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 85923149 | HCID 85923149 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11298265 | HCID 11298265 | 89.1% |
Reaction Steps
To a solution in ethyl acetate (20.0 mL) of the compound (634 mg) obtained in step (1) above, 20% palladium hydroxide/carbon (63.0 mg) was added. The mixture was stirred at room temperature for an hour in a hydrogen atmosphere. After passing the reaction mixture through Celite (registered trademark), the filtrate was concentrated under reduced pressure to give the titled compound as a pale yellow oil (320 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422240B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-4de129214d8849029ad4025fd67ef0c4 |
| Source note | uspto-grants-2016_08 |