Methylamine → N'-(4-Bromophenyl)-N-methyl-methanesulfonimidamide

HRID 1485609Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][CH:3]=1.[CH3:12][NH2:13]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[S:9]([CH3:11])([NH:13][CH3:12])=[O:10])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 6329Methylamine

HCID 14195208N-(4-Bromophenyl)methanesulfinamide

Product 1

HCID 118863941N'-(4-Bromophenyl)-N-methyl-methanesulfonimidamide

Procedure

The title compound is prepared from N-(4-bromophenyl)methanesulfinamide and methylamine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.85 min; Mass spectrum (ESI+): m/z=263, 265 [M+H]+.

Sources & evidence

ORD record: ord-f1b6f9a88cdd4abeb4c37352b58f436f
Source dataset: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09422312B2

Reaction notes

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