HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → 4-Bromo-N-[methyl(oxo)pyrrolidin-1-yl-lambda6-sulfanylidene]aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | N-(4-Bromophenyl)methanesulfinamide | HCID 14195208 | — |
| Product | 4-Bromo-N-[methyl(oxo)pyrrolidin-1-yl-lambda6-sulfanylidene]aniline | HCID 118863931 | — |
Reaction Steps
The title compound is prepared from N-(4-bromophenyl)methanesulfinamide and pyrrolidine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.99 min; Mass spectrum (ESI+): m/z=303, 305 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422312B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-01ee8290829c463a990902f8340a016b |
| Source note | uspto-grants-2016_08 |