HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfinyl chloride → HCID 118863919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfinyl chloride | HCID 548463 | — |
| Reactant | 2-Chloropyrimidin-5-amine | HCID 12215993 | — |
| Product | HCID 118863919 | HCID 118863919 | — |
Reaction Steps
The title compound is prepared from 5-amino-2-chloropyrimidine and methanesulfinyl chloride following a procedure analogous to that described for Intermediate 3 (Step 1). The reaction mixture is cooled in an ice bath for the entire reaction time. LC (method 1): tR=0.49 min; Mass spectrum (ESI+): m/z=192 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422312B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-dd69d225ad7c4c8486c5f97251f2cc94 |
| Source note | uspto-grants-2016_08 |