Methylamine → HCID 118863929, compound

HRID 1485640Notes

Reaction equation

HRID 1485640 reaction equation
[CH3:1][NH:2][S:3]([C:5]1[CH:10]=[CH:9][C:8]([Br:11])=[CH:7][CH:6]=1)=[O:4].[CH3:12][NH2:13]>>[Br:11][C:8]1[CH:9]=[CH:10][C:5]([S:3](=[N:13][CH3:12])([NH:2][CH3:1])=[O:4])=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 6329MethylamineHCID 118863953HCID 118863953, compound

Product 1

HCID 118863929HCID 118863929, compound

Procedure

The title compound is prepared from 4-bromo-benzenesulfinic acid methylamide and methylamine following a procedure analogous to that described for Intermediate 17 (Step 2). LC (method 1): tR=0.70 min; Mass spectrum (ESI+): m/z=263, 265 [M+H]+.

Sources & evidence

ORD record
ord-d916232481e34690baf623b7929529f0
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

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