Sodium Hydroxide → HCID 117834224, compound

Participants

Reaction Conditions

Reaction Steps

RBF was charged with 1200 ml of water and 15.01 gms of sodium hydroxide at 20-25° C. and stirred to get a clear solution. 100 gms of 3,5-Diiodotyrosine dihydrate was added and to the above mixture and stirred for an hour to get a clear solution. Copper sulphate solution (35.94 gms dissolved in 225 ml of water at 40° C.) was then added into the reaction mixture over a period of 1 hr and maintained at 20-25° C. for 1 hr. The resultant reaction mixture is filtered and washed with 1500 ml of DM water and dried under vacuum at 55-60° C. to get 95 gms of 3,5-Diiodo L-Tyrosine copper complex. The purity of obtained complex is NLT 97% with yield of 93-98%.

Provenance & Evidence