HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 117920437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 89881791 | HCID 89881791 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 117920437 | HCID 117920437 | — |
Reaction Steps
In addition, an oily product Compound 12 was dissolved in methylene chloride, and treated with hydrogen chloride-dioxane, to produce 1-((E)-2-decenoyl)-4-dimethylaminopiperidine hydrochloride (crystals, mp 185°-188° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428477B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-48c6f4eb640d43b2adfda5dd5a0228b4 |
| Source note | uspto-grants-2016_08 |